PBT603 - POLYMER CHARACTERIZATION LABORATORY

Course Name Code Semester Theory
(hours/week)
Application
(hours/week)
Credit ECTS
POLYMER CHARACTERIZATION LABORATORY PBT603 1st Semester 2 2 3 8
Prequisites
Course languageTurkish
Course typeElective 
Mode of DeliveryFace-to-Face 
Learning and teaching strategiesDiscussion
Demonstration
 
Instructor (s)Prof. Dr. Murat ÅžEN /Doç. Dr. Murat Barsbay  
Course objective The main aim of this course is teaching of the students for the characterization and analyses by using spectroscopic, chromatographic, thermal and mechanical instrumentation techniques in laboratory via experimental studies.  
Learning outcomes
  1. Student will learn the following subjects; 1. Copolymer analyses by FTIR 2. Molecular weight determination techniques 3. Flow behaviors in polymers shear thinning and shear thickening 4. Determination of additives and composition of polymers by TGA 5. Phase transitions in polymers i.e. Tg, Tm and Tc 6. Nano dimensions of polymer coils 7. Crystallinity in polymers and crystallinity determination techniques
Course ContentDetermination of acrylonitrile ratio in acrylic fabrics, Determination of molecular weight of water soluble polymers by Size exclusion chromatography, Rheological characterization of food additive natural polymers, Determination of PVC and carbon
black ratio in water pipes by TGA, Identification of phase transitions by DSC, Determination of polymer crystallization kinetics by dilatometer technique, Determination of nano dimensions of polymer coils by static light scattering technique, Determination of hydrophobicity/hydrophilicity of self?cleaning textiles by contact angle measurements, Investigation of strain?stress behaviors of thermoplastics and elastomeric polymers, Identification of shape memory of polymeric sponges by compression analyses, Determination of nano voids in polymers by positron annihilation lifetime spectrometer, Surface modification of demin fabrics by plasma technique
 
References? Arza Seidel, Characterization and Analysis of Polymers, John Wiley & Sons, 2008
? Barbara H. Stuart, Polymer Analysis, John Wiley & Sons, 2002
? Nicholas P. Cheremisinoff, Polymer Characterization: Laboratory Techniques and Analysis, Univ. Press of Mississippi, 1996.
? Thomas Roy, Introduction to Polymer Analysis, Crompton, iSmithers, 2009.
 

Course outline weekly

WeeksTopics
Week 1Determination of acrylonitrile ratio in acrylic fabrics
Week 2Determination of molecular weight of water soluble polymers by end group analyses
Week 3Determination of molecular weight by viscosimetric analyses
Week 4Rheological characterization of food additive natural polymers
Week 5Determination of PVC and carbon black ratio in water pipes by TGA
Week 6Midterm exam
Week 7Identification of phase transitions by DSC
Week 8Determination of polymer crystallization kinetics by dilatometer technique.
Week 9Determination of nano dimensions of polymer coils by static/dynamic light scattering technique.
Week 10Determination of hydrophobicity/hydrophilicity of self-cleaning textiles by contact angle measurements
Week 11Investigation of strain-stress behaviors of thermoplastics and elastomeric polymers
Week 12Identification of shape memory of polymeric sponges by compression analyses
Week 13Midterm exam
Week 14Determination of nano voids in polymers by positron annihilation lifetime spectrometer
Week 15Homework
Week 16Final exam

Assesment methods

Course activitiesNumberPercentage
Attendance00
Laboratory1340
Application00
Field activities00
Specific practical training00
Assignments00
Presentation00
Project00
Seminar00
Midterms220
Final exam140
Total100
Percentage of semester activities contributing grade succes050
Percentage of final exam contributing grade succes050
Total100

WORKLOAD AND ECTS CALCULATION

Activities Number Duration (hour) Total Work Load
Course Duration (x14) 0 0 0
Laboratory 13 4 52
Application000
Specific practical training000
Field activities000
Study Hours Out of Class (Preliminary work, reinforcement, ect)13678
Presentation / Seminar Preparation000
Project000
Homework assignment14040
Midterms (Study duration)13030
Final Exam (Study duration) 14040
Total Workload29120240

Matrix Of The Course Learning Outcomes Versus Program Outcomes

D.9. Key Learning OutcomesContrubition level*
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*1 Lowest, 2 Low, 3 Average, 4 High, 5 Highest