PBT602 - CHARACTERIZATION and ANALYSIS of POLYMERS

Course Name Code Semester Theory
(hours/week)
Application
(hours/week)
Credit ECTS
CHARACTERIZATION and ANALYSIS of POLYMERS PBT602 1st Semester 3 0 3 8
Prequisites
Course languageTurkish
Course typeElective 
Mode of DeliveryFace-to-Face 
Learning and teaching strategiesDiscussion
Demonstration
 
Instructor (s)Prof. Dr. Olgun Güven / Prof. Dr. Murat Åžen  
Course objectiveThe main aim of this course is training of the students on the basic instrumentation techniques on the characterization of chemical and physical properties of polymers.  
Learning outcomes
  1. Students satisfactorily completing the course will acquire the basic information for the characterization and test methods for identification of composition of polymers. Among various properties and methods relevant to their determination the following can be listed; various molecular weight averages and distributions, experimental techniques, data evaluation for colligative property measurements, osmotic pressure, light scattering, viscosimetry, size exclusion chromatography.
Course ContentSolubility of polymers, selection of a solvent, Molecular weight averages and distribution Colligative properties and determination of number average molecular weight, Light scattering and determination of weight average molecular weight
Solution viscosity and determination of viscosity average molecular weight, Size exclusion chromatography, Mechanical properties, elastic modulus, yield stress, elongation at break, toughness, Thermal properties, melting, crystallization, glass transition
Surface properties, contact angle, Pulse NMR, crosslink density crystallinity and stage of the water in polymer, Rheological properties and flow behaviors, storage and lost modules , Dielectric Relaxation
 
ReferencesCharacterization and Analysis of Polymers, Clavier, Ron, Wiley and Sons
Experimental Methods in Polymer Chemistry, Jan Rabek, Wiley Int. Ed., New York
Polymer Characterization, D. Campbell, R.A. Pethrick, J.R. White, Stanley Thornes, Cornwall.
Introduction to Physical Polymer Science, L.H. Sperling Wiley?Interscience, New York
 

Course outline weekly

WeeksTopics
Week 1Introduction : Characterization of Polymers, Test Methods for Composition
Week 2Types of molecular weight averages
Week 3Determination of molecular weight by colligative properties
Week 4Light Scattering
Week 5Size exclusion chromatography, homework
Week 6Pulse Nuclear Magnetic Resonance and Mass Spectrometry
Week 7Mid?term exam
Week 8Static mechanical properties
Week 9Dynamic mechanical properties
Week 10Thermal properties
Week 11Morphology and Topology
Week 12Surface properties, contact angle
Week 13Rheological Measurements.
Week 14Dielectric Relaxation
Week 15Homework
Week 16Final exam

Assesment methods

Course activitiesNumberPercentage
Attendance00
Laboratory00
Application00
Field activities00
Specific practical training00
Assignments220
Presentation00
Project00
Seminar00
Midterms130
Final exam150
Total100
Percentage of semester activities contributing grade succes050
Percentage of final exam contributing grade succes050
Total100

WORKLOAD AND ECTS CALCULATION

Activities Number Duration (hour) Total Work Load
Course Duration (x14) 14 3 42
Laboratory 0 0 0
Application000
Specific practical training000
Field activities000
Study Hours Out of Class (Preliminary work, reinforcement, ect)10660
Presentation / Seminar Preparation000
Project000
Homework assignment17070
Midterms (Study duration)13030
Final Exam (Study duration) 14040
Total Workload27149242

Matrix Of The Course Learning Outcomes Versus Program Outcomes

D.9. Key Learning OutcomesContrubition level*
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*1 Lowest, 2 Low, 3 Average, 4 High, 5 Highest